Information card for entry 4069068

Structure parameters

• Common name: (4-TMS-Ar*ZnH)2
• Formula: C96 H157.98 I0.02 Si2 Zn2
• Calculated formula: C96 H157.98 I0.02 Si2 Zn2
• Title of publication: Steric Enhancement of Group 12 Metal Hydride Stability and the Reaction of an Arylzinc Hydride with Tetramethylpiperidinyl Oxide (TEMPO)
• Authors of publication: Zhu, Zhongliang; Fettinger, James C.; Olmstead, Marilyn M.; Power, Philip P.
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 7
• Pages of publication: 2091
• a: 20.7441 ± 0.001 Å
• b: 17.1921 ± 0.0008 Å
• c: 28.8855 ± 0.0017 Å
• α: 90°
• β: 110.396 ± 0.001°
• γ: 90°
• Cell volume: 9655.7 ± 0.9 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.08
• Residual factor for significantly intense reflections: 0.0536
• Weighted residual factors for significantly intense reflections: 0.154
• Weighted residual factors for all reflections included in the refinement: 0.1663
• Goodness-of-fit parameter for all reflections included in the refinement: 1.09
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No