Information card for entry 4069150
| Formula |
C30.38 H43 Mg O4 |
| Calculated formula |
C30.375 H43 Mg O4 |
| Title of publication |
1,4-Dioxane Adducts of Grignard Reagents: Synthesis, Ether Fragmentation Reactions, and Structural Diversity of Grignard Reagent/1,4-Dioxane Complexes |
| Authors of publication |
Langer, Jens; Krieck, Sven; Fischer, Reinald; Görls, Helmar; Walther, Dirk; Westerhausen, Matthias |
| Journal of publication |
Organometallics |
| Year of publication |
2009 |
| Journal volume |
28 |
| Journal issue |
19 |
| Pages of publication |
5814 |
| a |
11.9417 ± 0.0002 Å |
| b |
25.0853 ± 0.0003 Å |
| c |
20.1698 ± 0.0003 Å |
| α |
90° |
| β |
91.963 ± 0.001° |
| γ |
90° |
| Cell volume |
6038.54 ± 0.15 Å3 |
| Cell temperature |
183 ± 2 K |
| Ambient diffraction temperature |
183 ± 2 K |
| Number of distinct elements |
4 |
| Space group number |
14 |
| Hermann-Mauguin space group symbol |
P 1 21/n 1 |
| Hall space group symbol |
-P 2yn |
| Residual factor for all reflections |
0.1147 |
| Residual factor for significantly intense reflections |
0.0673 |
| Weighted residual factors for significantly intense reflections |
0.1765 |
| Weighted residual factors for all reflections included in the refinement |
0.21 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.017 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
Yes |
| Has Fobs |
No |
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https://www.crystallography.net/4069150.html
