Information card for entry 4069409

Structure parameters

• Formula: C14 H39 Ge I Si4
• Calculated formula: C14 H39 Ge I Si4
• SMILES: [GeH](I)(C([Si](C)(C)C)[Si](C)(C)C)C([Si](C)(C)C)[Si](C)(C)C
• Title of publication: Silylene- and Germylene-Mediated C−H Activation: Reaction with Alkanes, Ethers, and Amines
• Authors of publication: Walker, Randon H.; Miller, Karla A.; Scott, Sara L.; Cygan, Zuzanna T.; Bartolin, Jeffrey M.; Kampf, Jeff W.; Banaszak Holl, Mark M.
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 9
• Pages of publication: 2744
• a: 9.2067 ± 0.001 Å
• b: 21.527 ± 0.002 Å
• c: 13.1974 ± 0.0014 Å
• α: 90°
• β: 110.055 ± 0.002°
• γ: 90°
• Cell volume: 2457 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0192
• Residual factor for significantly intense reflections: 0.0189
• Weighted residual factors for significantly intense reflections: 0.0502
• Weighted residual factors for all reflections included in the refinement: 0.0504
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No