Information card for entry 4069470

Structure parameters

• Formula: C434 H356 Bi40 N56 O281
• Calculated formula: C434 H344 Bi40 N56 O281
• Title of publication: Synthesis, Ethanolysis, and Hydrolysis of Bismuth(III)ortho-Nitrobenzoate Complexes en Route to a Pearl Necklace-like Polymer of Bi10Oxo-Clusters
• Authors of publication: Andrews, Philip C.; Deacon, Glen B.; Junk, Peter C.; Kumar, Ish; MacLellan, Jonathan G.
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 14
• Pages of publication: 3999
• a: 17.6559 ± 0.0006 Å
• b: 21.422 ± 0.0007 Å
• c: 35.9678 ± 0.0011 Å
• α: 89.761 ± 0.002°
• β: 89.313 ± 0.002°
• γ: 87.692 ± 0.002°
• Cell volume: 13591.8 ± 0.8 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1377
• Residual factor for significantly intense reflections: 0.063
• Weighted residual factors for significantly intense reflections: 0.1321
• Weighted residual factors for all reflections included in the refinement: 0.1576
• Goodness-of-fit parameter for all reflections included in the refinement: 0.988
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No