Information card for entry 4069676

Structure parameters

• Formula: C28 H30 Cl N3 O Rh
• Calculated formula: C28 H30 Cl N3 O0.5 Rh
• Title of publication: First Examples of Heteroleptic Dipyrrin/η5-Pentamethylcyclopentadienyl Rhodium/Iridium(III) Complexes and Their Catalytic Activity
• Authors of publication: Yadav, Mahendra; Singh, Ashish Kumar; Pandey, Daya Shankar
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 16
• Pages of publication: 4713
• a: 16.047 ± 0.004 Å
• b: 16.61 ± 0.004 Å
• c: 19.215 ± 0.004 Å
• α: 90°
• β: 99.379 ± 0.004°
• γ: 90°
• Cell volume: 5053 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.038
• Residual factor for significantly intense reflections: 0.0322
• Weighted residual factors for significantly intense reflections: 0.076
• Weighted residual factors for all reflections included in the refinement: 0.0784
• Goodness-of-fit parameter for all reflections included in the refinement: 1.121
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No