Information card for entry 4069736

Structure parameters

• Formula: C25 H39 Cl7 N4 Rh Sn2
• Calculated formula: C26 H40 Cl10 N4 Rh Sn2
• SMILES: c12c3cccc1C[N](C)(C)[Sn]2([N](C3)(C)C)(Cl)[Rh](Cl)(Cl)[Sn]12(c3c(cccc3C[N]2(C)C)C[N]1(C)C)Cl.C(Cl)(Cl)Cl.C(Cl)(Cl)Cl
• Title of publication: The Stannylene {2,6-(Me2NCH2)2C6H3}SnCl as a Ligand in Transition Metal Complexes of Palladium, Ruthenium, and Rhodium
• Authors of publication: Martincová, Jana; Dostálová, Romana; Dostál, Libor; Růžička, Aleš; Jambor, Roman
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 16
• Pages of publication: 4823
• a: 12.295 ± 0.0007 Å
• b: 12.194 ± 0.0009 Å
• c: 16.497 ± 0.0005 Å
• α: 90°
• β: 127.008 ± 0.004°
• γ: 90°
• Cell volume: 1975.1 ± 0.2 ų
• Cell temperature: 150 ± 1 K
• Ambient diffraction temperature: 150 ± 1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0502
• Residual factor for significantly intense reflections: 0.039
• Weighted residual factors for significantly intense reflections: 0.0859
• Weighted residual factors for all reflections included in the refinement: 0.0936
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No