Information card for entry 4070171

Structure parameters

• Chemical name: 1,1-bis[kappa-O,N-(8-oxyquinolinato)]silacyclopentane THF-hemisolvate
• Formula: C48 H48 N4 O5 Si2
• Calculated formula: C48 H48 N4 O5 Si2
• Title of publication: Hypercoordinate Silacycloalkanes: Step-by-Step Tuning of N→Si Interactions§
• Authors of publication: Brendler, Erica; Wächtler, Erik; Wagler, Jörg
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 18
• Pages of publication: 5459
• a: 32.107 ± 0.002 Å
• b: 8.2085 ± 0.0006 Å
• c: 19.9681 ± 0.0015 Å
• α: 90°
• β: 127.929 ± 0.003°
• γ: 90°
• Cell volume: 4151 ± 0.5 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0854
• Residual factor for significantly intense reflections: 0.0407
• Weighted residual factors for significantly intense reflections: 0.0877
• Weighted residual factors for all reflections included in the refinement: 0.0985
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No