Information card for entry 4070346

Structure parameters

• Formula: C28 H52 Al B N6 Yb
• Calculated formula: C28 H52 Al B N6 Yb
• SMILES: [Yb]123([n]4n(c(cc4C(C)(C)C)C)[BH](n4[n]1c(cc4C)C(C)(C)C)n1[n]2c(cc1C)C(C)(C)C)[CH3][Al]([CH3]3)(C)C
• Title of publication: Monomeric Tetraalkylaluminates of Divalent Ytterbium Stabilized by a Bulky Tris(pyrazolyl)borate Ligand
• Authors of publication: Litlabø, Rannveig; Saliu, Kuburat; Ferguson, Michael J.; McDonald, Robert; Takats, Josef; Anwander, Reiner
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 23
• Pages of publication: 6750
• a: 11.8519 ± 0.0004 Å
• b: 12.6876 ± 0.0005 Å
• c: 12.7193 ± 0.0005 Å
• α: 81.4737 ± 0.0004°
• β: 78.9276 ± 0.0004°
• γ: 64.2133 ± 0.0004°
• Cell volume: 1685.57 ± 0.11 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0289
• Residual factor for significantly intense reflections: 0.0238
• Weighted residual factors for significantly intense reflections: 0.0536
• Weighted residual factors for all reflections included in the refinement: 0.0556
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No