Crystallography Open Database

Information card for entry 4070493

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Coordinates	4070493.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H47 B F4 N2 P2 Pd
Calculated formula	C30 H47 B F4 N2 P2 Pd
Title of publication	A Cationic AgI(PNPtBu) Species Acting as PNP Transfer Agent: Facile Synthesis of Pd(PNPtBu)(alkyl) Complexes and Their Reactivity Compared to PCPtBuAnalogues
Authors of publication	van der Vlugt, Jarl Ivar; Siegler, Maxime A.; Janssen, Michèle; Vogt, Dieter; Spek, Anthony L.
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	24
Pages of publication	7025
a	33.9886 ± 0.0011 Å
b	11.0088 ± 0.0003 Å
c	19.8282 ± 0.0005 Å
α	90°
β	96.546 ± 0.002°
γ	90°
Cell volume	7370.8 ± 0.4 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0582
Residual factor for significantly intense reflections	0.036
Weighted residual factors for significantly intense reflections	0.077
Weighted residual factors for all reflections included in the refinement	0.0826
Goodness-of-fit parameter for all reflections included in the refinement	1.071
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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