Information card for entry 4070970

Structure parameters

• Formula: C72.5 H94 Lu N O2 P2 Si2
• Calculated formula: C72.5 H93.5 Lu N O2 P2 Si2
• Title of publication: Synthesis, Characterization, and Reactivity of the Thermally Stable Lutetium Tris(alkyl) Complex (tBu2bpy)Lu(CH2SiMe3)3
• Authors of publication: Masuda, Jason D.; Jantunen, Kimberly C.; Scott, Brian L.; Kiplinger, Jaqueline L.
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 6
• Pages of publication: 1299
• a: 13.882 ± 0.002 Å
• b: 14.506 ± 0.002 Å
• c: 17.549 ± 0.003 Å
• α: 94.916 ± 0.002°
• β: 103.589 ± 0.002°
• γ: 92.979 ± 0.002°
• Cell volume: 3412.8 ± 0.9 ų
• Cell temperature: 141 ± 2 K
• Ambient diffraction temperature: 141 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1434
• Residual factor for significantly intense reflections: 0.072
• Weighted residual factors for significantly intense reflections: 0.1286
• Weighted residual factors for all reflections included in the refinement: 0.1619
• Goodness-of-fit parameter for all reflections included in the refinement: 0.907
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No