Information card for entry 4072437

Structure parameters

• Formula: C35 H32 Ge O3
• Calculated formula: C35 H32 Ge O3
• SMILES: [Ge]1(OC2(OC(=O)C=C2)C21c1ccccc1c1ccccc21)(c1c(cc(cc1C)C)C)c1c(cc(cc1C)C)C
• Title of publication: Versatile Reactivity of the Germene Mes2GeCR2toward Esters and Related Carbonyl Derivatives
• Authors of publication: Ech-Cherif El Kettani, Sakina; Lazraq, Mohamed; Ranaivonjatovo, Henri; Escudié, Jean; Gornitzka, Heinz; Ouhsaine, Fatima
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 15
• Pages of publication: 3729
• a: 11.4843 ± 0.0007 Å
• b: 21.4191 ± 0.0013 Å
• c: 11.6183 ± 0.0007 Å
• α: 90°
• β: 103.808 ± 0.001°
• γ: 90°
• Cell volume: 2775.3 ± 0.3 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0338
• Residual factor for significantly intense reflections: 0.0284
• Weighted residual factors for significantly intense reflections: 0.0712
• Weighted residual factors for all reflections included in the refinement: 0.0738
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No