Information card for entry 4072571

Structure parameters

• Formula: C109.6 H98.4 Li4 N4 P4
• Calculated formula: C107.6 H84 Li4 N4 P4
• Title of publication: A Tetrameric Lithiated Phosphazene Containing a Lithium Atom Bound Exclusively to Four sp3-Hybridized Carbanionic Centers: A Key Intermediate for Understanding Structure−Reactivity Relationships of Phosphazenyllithium Compounds
• Authors of publication: Ruiz Gómez, Gloria; Fernández, Ignacio; López Ortiz, Fernando; Price, Richard D.; Davidson, Matthew G.; Mahon, Mary F.; Howard, Judith A. K.
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 3
• Pages of publication: 514
• a: 18.763 ± 0.004 Å
• b: 20.181 ± 0.004 Å
• c: 25.127 ± 0.005 Å
• α: 90°
• β: 104.52 ± 0.03°
• γ: 90°
• Cell volume: 9211 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1598
• Residual factor for significantly intense reflections: 0.0999
• Weighted residual factors for significantly intense reflections: 0.2391
• Weighted residual factors for all reflections included in the refinement: 0.2622
• Goodness-of-fit parameter for all reflections included in the refinement: 1.062
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No