Information card for entry 4072661

Structure parameters

• Formula: C30 H60 N4 O3 Os2 Pd Si4
• Calculated formula: C30 H60 N4 O3 Os2 Pd Si4
• SMILES: C([Os]12(C[Si](C)(C)C)(#N)[O]3[Os]4(C[Si](C)(C)C)(C[Si](C)(C)C)(#N)[O]1[Pd]1234[n]2ccccc2c2cccc[n]12)[Si](C)(C)C.O1CCCC1
• Title of publication: Synthesis, Structure, and Reactivity of Organometallic Osmium(VI) Hydroxo Compounds
• Authors of publication: Kiefer, Adam M.; Giles, John A.; Shapley, Patricia A.
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 8
• Pages of publication: 1881
• a: 12.35 ± 0.0009 Å
• b: 18.3598 ± 0.0013 Å
• c: 19.9189 ± 0.0013 Å
• α: 90°
• β: 101.883 ± 0.003°
• γ: 90°
• Cell volume: 4419.7 ± 0.5 ų
• Cell temperature: 297 ± 2 K
• Ambient diffraction temperature: 297 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0624
• Residual factor for significantly intense reflections: 0.0327
• Weighted residual factors for significantly intense reflections: 0.0641
• Weighted residual factors for all reflections included in the refinement: 0.0769
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No