Information card for entry 4073394
| Formula |
C24.5 H34 Cl2 O5 Sn |
| Calculated formula |
C24.5 H34 Cl2 O5 Sn |
| Title of publication |
Ph(3-n)XnSnCH2-16-crown-5 (X = F, Cl, Br, I, SCN;n= 1, 2): Intramolecular O →Sn Coordination versus Ditopic Complexation of Sodium Thiocyanate† |
| Authors of publication |
Reeske, Gregor; Schürmann, Markus; Costisella, Burkhard; Jurkschat, Klaus |
| Journal of publication |
Organometallics |
| Year of publication |
2007 |
| Journal volume |
26 |
| Journal issue |
17 |
| Pages of publication |
4170 |
| a |
9.316 ± 0.0006 Å |
| b |
12.6372 ± 0.0006 Å |
| c |
12.726 ± 0.0008 Å |
| α |
114.544 ± 0.003° |
| β |
99.695 ± 0.002° |
| γ |
96.533 ± 0.004° |
| Cell volume |
1314.87 ± 0.14 Å3 |
| Cell temperature |
173 ± 1 K |
| Ambient diffraction temperature |
173 ± 1 K |
| Number of distinct elements |
5 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0394 |
| Residual factor for significantly intense reflections |
0.0253 |
| Weighted residual factors for significantly intense reflections |
0.0412 |
| Weighted residual factors for all reflections included in the refinement |
0.0424 |
| Goodness-of-fit parameter for all reflections included in the refinement |
0.819 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
For the version history of this entry, please navigate to main COD server.
The link is:
https://www.crystallography.net/4073394.html
