Information card for entry 4073411

Structure parameters

• Formula: C32 H66 O Si6 Tm
• Calculated formula: C32 H66 O Si6 Tm
• SMILES: [Tm]12345678([O]9CCCC9)([c]9([cH]4[c]3([Si](C)(C)C)[cH]2[c]19[Si](C)(C)C)[Si](C)(C)C)[c]1([c]5([Si](C)(C)C)[cH]6[c]7([cH]81)[Si](C)(C)C)[Si](C)(C)C
• Title of publication: Synthesis and Reactivity of Organometallic Complexes of Divalent Thulium with Cyclopentadienyl and Phospholyl Ligands
• Authors of publication: Jaroschik, Florian; Nief, François; Le Goff, Xavier-Frédéric; Ricard, Louis
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 14
• Pages of publication: 3552
• a: 11.348 ± 0.001 Å
• b: 22.12 ± 0.001 Å
• c: 16.841 ± 0.001 Å
• α: 90°
• β: 97.75 ± 0.001°
• γ: 90°
• Cell volume: 4188.8 ± 0.5 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0628
• Residual factor for significantly intense reflections: 0.0364
• Weighted residual factors for significantly intense reflections: 0.0708
• Weighted residual factors for all reflections included in the refinement: 0.0772
• Goodness-of-fit parameter for all reflections included in the refinement: 0.998
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No