Information card for entry 4073509

Structure parameters

• Common name: 04224
• Formula: C30 H66 K2 O3 Si4
• Calculated formula: C30 H66 K2 O3 Si4
• Title of publication: Trimethylsilylated Allyl Complexes of the Heavy Alkali Metals, M[1,3-(SiMe3)2C3H3](thf)n(M = K, Cs)
• Authors of publication: Quisenberry, Keith T.; Gren, Cameron K.; White, Rosemary E.; Hanusa, Timothy P.; Brennessel, William W.
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 17
• Pages of publication: 4354
• a: 23.151 ± 0.002 Å
• b: 11.0862 ± 0.0009 Å
• c: 16.9491 ± 0.0014 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4350.1 ± 0.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.0559
• Residual factor for significantly intense reflections: 0.0422
• Weighted residual factors for significantly intense reflections: 0.1054
• Weighted residual factors for all reflections included in the refinement: 0.1177
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No