Information card for entry 4073622

Structure parameters

• Common name: [Zn3(TMG)4(Et)2] (1)
• Formula: C24 H58 N12 Zn3
• Calculated formula: C24 H58 N12 Zn3
• SMILES: [Zn]12([N]([Zn]([N]1=C(N(C)C)N(C)C)CC)=C(N(C)C)N(C)C)[N]([Zn]([N]2=C(N(C)C)N(C)C)CC)=C(N(C)C)N(C)C
• Title of publication: Synthesis, Structure, and Reactivity of Alkylzinc Complexes Stabilized with 1,1,3,3-Tetramethylguanidine
• Authors of publication: Bunge, Scott D.; Lance, Jacob M.; Bertke, Jeffrey A.
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 25
• Pages of publication: 6320
• a: 13.5902 ± 0.0013 Å
• b: 14.3845 ± 0.0013 Å
• c: 18.5827 ± 0.0017 Å
• α: 90°
• β: 101.762 ± 0.002°
• γ: 90°
• Cell volume: 3556.4 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1384
• Residual factor for significantly intense reflections: 0.0559
• Weighted residual factors for significantly intense reflections: 0.1216
• Weighted residual factors for all reflections included in the refinement: 0.1588
• Goodness-of-fit parameter for all reflections included in the refinement: 0.999
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No