Information card for entry 4073734

Structure parameters

• Formula: C22 H40 I2 O2 P Sm
• Calculated formula: C22 H40 I2 O2 P Sm
• SMILES: [Sm]1234([O]5CCCC5)([O]5CCCC5)(P5[C]1(=[C]2([C]3(=[C]45C(C)(C)C)C)C)C(C)(C)C)(I)I
• Title of publication: Synthesis, Characterization, and Reactivity of Mono(phospholyl)lanthanoid(III) Bis(dimethylaminobenzyl) Complexes
• Authors of publication: Jaroschik, Florian; Shima, Takanori; Li, Xiaofang; Mori, Kyouichi; Ricard, Louis; Le Goff, Xavier-Frédéric; Nief, François; Hou, Zhaomin
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 23
• Pages of publication: 5654
• a: 17.435 ± 0.002 Å
• b: 8.688 ± 0.001 Å
• c: 18.59 ± 0.003 Å
• α: 90°
• β: 96.765 ± 0.002°
• γ: 90°
• Cell volume: 2796.3 ± 0.6 ų
• Cell temperature: 163 ± 2 K
• Ambient diffraction temperature: 163 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0601
• Residual factor for significantly intense reflections: 0.0409
• Weighted residual factors for significantly intense reflections: 0.0859
• Weighted residual factors for all reflections included in the refinement: 0.0928
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No