Information card for entry 4073910

Structure parameters

• Common name: 1b
• Chemical name: 1b
• Formula: C27 H42 O Si2
• Calculated formula: C27 H42 O Si2
• SMILES: [SiH](C)(C)c1cc(cc2c1Oc1c([SiH](C)C)cc(cc1C2(C)C)C(C)(C)C)C(C)(C)C
• Title of publication: Iron, Ruthenium, and Osmium Complexes Supported by the Bis(silyl) Chelate Ligand (9,9-Dimethylxanthene-4,5-diyl)bis(dimethylsilyl): Synthesis, Characterization, and Reactivity
• Authors of publication: Minglana, Jim Josephus G.; Okazaki, Masaaki; Hasegawa, Kenji; Luh, Lung-Shiang; Yamahira, Nobukazu; Komuro, Takashi; Ogino, Hiroshi; Tobita, Hiromi
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 24
• Pages of publication: 5859
• a: 10.319 ± 0.004 Å
• b: 10.579 ± 0.003 Å
• c: 13.042 ± 0.003 Å
• α: 90°
• β: 97.83 ± 0.02°
• γ: 90°
• Cell volume: 1410.5 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.1032
• Residual factor for significantly intense reflections: 0.0542
• Weighted residual factors for significantly intense reflections: 0.1355
• Weighted residual factors for all reflections included in the refinement: 0.1597
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No