Information card for entry 4074017

Structure parameters

• Formula: C35 H62.5 N Nb O0.25 P2 Si2
• Calculated formula: C35 H62.5 N Nb O0.25 P2 Si2
• Title of publication: Niobium Bis-alkylidene Complexes Prepared by a Multi-Electron Redox Process
• Authors of publication: Kilgore, Uriah J.; Tomaszewski, John; Fan, Hongjun; Huffman, John C.; Mindiola, Daniel J.
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 25
• Pages of publication: 6132
• a: 11.302 ± 0.0013 Å
• b: 11.7003 ± 0.0013 Å
• c: 31.275 ± 0.004 Å
• α: 82.957 ± 0.003°
• β: 81.382 ± 0.003°
• γ: 77.863 ± 0.003°
• Cell volume: 3979.8 ± 0.8 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0582
• Residual factor for significantly intense reflections: 0.0365
• Weighted residual factors for significantly intense reflections: 0.0921
• Weighted residual factors for all reflections included in the refinement: 0.1008
• Goodness-of-fit parameter for all reflections included in the refinement: 0.983
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No