Information card for entry 4074104

Structure parameters

• Formula: C73 H61 Cl13 N8 O5 Ru2
• Calculated formula: C72.532 H60.064 Cl13 N8 O5.258 Ru2
• Title of publication: Negishi CouplingExpedient Formation of Biphenyls on the Periphery of Inorganic/Organometallic Diruthenium Species
• Authors of publication: Zhang, Lei; Huang, Zhihong; Chen, Wei-Zhong; Negishi, Ei-ichi; Fanwick, Phillip E.; Updegraff, James B.; Protasiewicz, John D.; Ren, Tong
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 26
• Pages of publication: 6526
• a: 16.1963 ± 0.0002 Å
• b: 18.3611 ± 0.0003 Å
• c: 27.7087 ± 0.0004 Å
• α: 88.5192 ± 0.0006°
• β: 75.1286 ± 0.0005°
• γ: 77.435 ± 0.0008°
• Cell volume: 7769.4 ± 0.2 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.084
• Residual factor for significantly intense reflections: 0.058
• Weighted residual factors for significantly intense reflections: 0.141
• Weighted residual factors for all reflections included in the refinement: 0.155
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MO-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No