Information card for entry 4074628

Structure parameters

• Formula: C10 H22 B8 Co P
• Calculated formula: C10 H22 B8 Co P
• Title of publication: (Tetramethylcyclobutadiene)cobalt Complexes with Phosphacarborane Ligands†
• Authors of publication: Mutseneck, Elena V.; Perekalin, Dmitry S.; Holub, Josef; Starikova, Zoya A.; Petrovskii, Pavel V.; Zanello, Piero; Corsini, Maddalena; Štíbr, Bohumil; Kudinov, Alexander R.
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 10
• Pages of publication: 2419
• a: 7.176 ± 0.0017 Å
• b: 16.922 ± 0.004 Å
• c: 13.252 ± 0.003 Å
• α: 90°
• β: 101.582 ± 0.017°
• γ: 90°
• Cell volume: 1576.5 ± 0.6 ų
• Cell temperature: 163 ± 2 K
• Ambient diffraction temperature: 163 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0445
• Residual factor for significantly intense reflections: 0.0324
• Weighted residual factors for significantly intense reflections: 0.0693
• Weighted residual factors for all reflections included in the refinement: 0.0732
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No