Information card for entry 4074752

Structure parameters

• Formula: C61 H31 B F20 N2 P Rh Si
• Calculated formula: C61 H31 B F20 N2 P Rh Si
• SMILES: [RhH]12([P](c3ccccc3)(c3ccccc3)c3ccccc3)[Si](c3cccc4ccc[n]1c34)(c1cccc3ccc[n]2c13)C.Fc1c(c(F)c(F)c(F)c1F)[B-](c1c(F)c(F)c(F)c(F)c1F)(c1c(F)c(F)c(F)c(F)c1F)c1c(F)c(F)c(F)c(F)c1F
• Title of publication: Rhodium Complexes Containing a Tridentate Bis(8-quinolyl)methylsilyl Ligand: Synthesis and Reactivity
• Authors of publication: Sangtrirutnugul, Preeyanuch; Stradiotto, Mark; Tilley, T. Don
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 7
• Pages of publication: 1607
• a: 13.978 ± 0.001 Å
• b: 15.035 ± 0.001 Å
• c: 15.397 ± 0.001 Å
• α: 89.736 ± 0.001°
• β: 72 ± 0.001°
• γ: 88.186 ± 0.001°
• Cell volume: 3075.9 ± 0.4 ų
• Cell temperature: 117.2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.071
• Residual factor for significantly intense reflections: 0.0711
• Weighted residual factors for all reflections: 0.1167
• Weighted residual factors for all reflections included in the refinement: 0.1167
• Goodness-of-fit parameter for all reflections included in the refinement: 3.661
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No