Information card for entry 4075030

Structure parameters

• Chemical name: bis[mu3-(eta2/eta2/eta2-[2.2.2]paracyclophane)]- tris[tetra(mu2-trifluoroacetato-O,O')-dirhodium(II,II)]
• Formula: C72 H48 F36 O24 Rh6
• Calculated formula: C72 H48 F36 O24 Rh6
• Title of publication: Paracyclophanes as Versatileπ-Donor Ligands Directing Formation of Extended Organometallic Networks
• Authors of publication: Petrukhina, Marina A.; Filatov, Alexander S.; Sevryugina, Yulia; Andreini, Kristian W.; Takamizawa, Satoshi
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 9
• Pages of publication: 2135
• a: 20.5186 ± 0.0005 Å
• b: 20.5186 ± 0.0005 Å
• c: 17.7415 ± 0.0009 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 6468.7 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 166
• Hermann-Mauguin space group symbol: R -3 m :H
• Hall space group symbol: -R 3 2"
• Residual factor for all reflections: 0.05
• Residual factor for significantly intense reflections: 0.0442
• Weighted residual factors for significantly intense reflections: 0.1109
• Weighted residual factors for all reflections included in the refinement: 0.1162
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No