Information card for entry 4075084

Structure parameters

• Formula: C108 H172 Cl4 Cu4 Ge4 I4 N8 O8 Si8
• Calculated formula: C108 H172 Cl4 Cu4 Ge4 I4 N8 O8 Si8
• SMILES: C[Si](C1=C(N([Ge@@](Cl)([Cu]23[I]4[Cu]5([I]2[Cu]2([I]3[Cu]4([I]52)[Ge@@]2([n]3ccccc3C(=C(N2[Si](C)(C)C)c2ccccc2)[Si](C)(C)C)Cl)[Ge@@]2([n]3ccccc3C(=C(N2[Si](C)(C)C)c2ccccc2)[Si](C)(C)C)Cl)[Ge@]2([n]3ccccc3C(=C(N2[Si](C)(C)C)c2ccccc2)[Si](C)(C)C)Cl)[n]2ccccc12)[Si](C)(C)C)c1ccccc1)(C)C.O1CCCC1.O1CCCC1.O1CCCC1.O1CCCC1.O1CCCC1.O1CCCC1.O1CCCC1.O1CCCC1
• Title of publication: Reactivity of Pyridyl-1-azaallyl Germanium(II) Chloride: Synthesis of Novel Lithium Germinate [{(PhC⋮C)3Ge}3GeLi(Et2O)3] and Ge(II)−M(I) (M = Cu and Au) Adducts
• Authors of publication: Leung, Wing-Por; So, Cheuk-Wai; Chong, Kim-Hung; Kan, Kwok-Wai; Chan, Hoi-Shan; Mak, Thomas C. W.
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 11
• Pages of publication: 2851
• a: 22.2933 ± 0.0008 Å
• b: 22.2933 ± 0.0008 Å
• c: 14.1706 ± 0.0007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7042.7 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 9
• Space group number: 114
• Hermann-Mauguin space group symbol: P -4 21 c
• Hall space group symbol: P -4 2n
• Residual factor for all reflections: 0.1191
• Residual factor for significantly intense reflections: 0.0509
• Weighted residual factors for significantly intense reflections: 0.1132
• Weighted residual factors for all reflections included in the refinement: 0.1467
• Goodness-of-fit parameter for all reflections included in the refinement: 0.916
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No