Information card for entry 4075089

Structure parameters

• Formula: C84 H75 Ge4 Li O3
• Calculated formula: C84 H75 Ge4 Li O3
• SMILES: [Ge]([Ge]([Ge](C#Cc1ccccc1)(C#Cc1ccccc1)C#Cc1ccccc1)([Ge](C#Cc1ccccc1)(C#Cc1ccccc1)C#Cc1ccccc1)[Li]([O](CC)CC)([O](CC)CC)[O](CC)CC)(C#Cc1ccccc1)(C#Cc1ccccc1)C#Cc1ccccc1
• Title of publication: Reactivity of Pyridyl-1-azaallyl Germanium(II) Chloride: Synthesis of Novel Lithium Germinate [{(PhC⋮C)3Ge}3GeLi(Et2O)3] and Ge(II)−M(I) (M = Cu and Au) Adducts
• Authors of publication: Leung, Wing-Por; So, Cheuk-Wai; Chong, Kim-Hung; Kan, Kwok-Wai; Chan, Hoi-Shan; Mak, Thomas C. W.
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 11
• Pages of publication: 2851
• a: 15.4011 ± 0.0007 Å
• b: 24.5315 ± 0.0011 Å
• c: 21.9725 ± 0.001 Å
• α: 90°
• β: 99.8 ± 0.001°
• γ: 90°
• Cell volume: 8180.3 ± 0.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1985
• Residual factor for significantly intense reflections: 0.0812
• Weighted residual factors for significantly intense reflections: 0.2376
• Weighted residual factors for all reflections included in the refinement: 0.278
• Goodness-of-fit parameter for all reflections included in the refinement: 0.942
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No