Crystallography Open Database

Information card for entry 4075324

Preview

Coordinates	4075324.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H60 B20 Ru2 Si2
Calculated formula	C30 H60 B20 Ru2 Si2
Title of publication	Reaction of [η5:σ-Me2C(C5H4)(C2B10H10)]Ru(NCCH3)2with Me3SiC⋮CR. Synthesis and Structural Characterization of Mononuclear Ruthenium Bis(vinylidene) and Vinylvinylidene Complexes
Authors of publication	Sun, Yi; Chan, Hoi-Shan; Dixneuf, Pierre H.; Xie, Zuowei
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	11
Pages of publication	2719
a	18.2566 ± 0.0009 Å
b	10.5525 ± 0.0005 Å
c	22.7478 ± 0.0011 Å
α	90°
β	90.27 ± 0.001°
γ	90°
Cell volume	4382.4 ± 0.4 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0383
Residual factor for significantly intense reflections	0.0275
Weighted residual factors for significantly intense reflections	0.0696
Weighted residual factors for all reflections included in the refinement	0.0735
Goodness-of-fit parameter for all reflections included in the refinement	1.048
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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