Information card for entry 4075596

Structure parameters

• Formula: C113.5 H95 O3 P3 Pt3 Si3
• Calculated formula: C113.5 H91 O3 P3 Pt3 Si3
• Title of publication: Si−H Bond Activation by (Ph3P)2Pt(η2-C2H4) in Dihydrosilicon Tricycles that Also Contain O and N Heteroatoms
• Authors of publication: Braddock-Wilking, Janet; Corey, Joyce Y.; French, Lisa M.; Choi, Eunwoo; Speedie, Victoria J.; Rutherford, Michael F.; Yao, Shu; Xu, Huan; Rath, Nigam P.
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 16
• Pages of publication: 3974
• a: 14.0065 ± 0.0003 Å
• b: 14.0128 ± 0.0003 Å
• c: 26.8447 ± 0.0006 Å
• α: 85.955 ± 0.001°
• β: 78.652 ± 0.001°
• γ: 66.771 ± 0.001°
• Cell volume: 4746.9 ± 0.18 ų
• Cell temperature: 165 ± 2 K
• Ambient diffraction temperature: 165 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1735
• Residual factor for significantly intense reflections: 0.057
• Weighted residual factors for significantly intense reflections: 0.0894
• Weighted residual factors for all reflections included in the refinement: 0.1238
• Goodness-of-fit parameter for all reflections included in the refinement: 0.957
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No