Information card for entry 4075676

Structure parameters

• Formula: C102 H116 P4 Pt2
• Calculated formula: C102 H116 P4 Pt2
• Title of publication: Selective Metallacyclization and Crystallographic Characterization of Structurally Related Platina-annulenes
• Authors of publication: Johnson, Charles A.; Haley, Michael M.; Rather, Elisabeth; Han, Fusen; Weakley, Timothy J. R.
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 6
• Pages of publication: 1161
• a: 13.6001 ± 0.0016 Å
• b: 13.7981 ± 0.0016 Å
• c: 14.8932 ± 0.0018 Å
• α: 76.349 ± 0.002°
• β: 62.971 ± 0.002°
• γ: 81.647 ± 0.002°
• Cell volume: 2416.9 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0911
• Residual factor for significantly intense reflections: 0.0523
• Weighted residual factors for significantly intense reflections: 0.1068
• Weighted residual factors for all reflections included in the refinement: 0.1211
• Goodness-of-fit parameter for all reflections included in the refinement: 0.993
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No