Information card for entry 4075800

Structure parameters

• Chemical name: (μ~2~-bromo)bis((η^3^-allyl)(triisopropylphosphine)nickel) tetra(nonafluoro-tetrabutoxy)aluminate
• Formula: C40 H52 Al Br F36 Ni2 O4 P2
• Calculated formula: C40 H52 Al Br F36 Ni2 O4 P2
• Title of publication: Dinuclear [{(π-C3H5)M(PR3)}2(μ-X)]Y Complexes of Nickel and Palladium†
• Authors of publication: Alberti, Davide; Goddard, Richard; Pörschke, Klaus-Richard
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 16
• Pages of publication: 3907
• a: 15.0314 ± 0.0003 Å
• b: 17.5337 ± 0.0002 Å
• c: 22.1486 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5837.4 ± 0.17 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 8
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0614
• Residual factor for significantly intense reflections: 0.0427
• Weighted residual factors for significantly intense reflections: 0.0752
• Weighted residual factors for all reflections included in the refinement: 0.0814
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No