Information card for entry 4076070

Structure parameters

• Formula: C10 H18 Cl3 N2 Nb Si
• Calculated formula: C10 H18 Cl3 N2 Nb Si
• SMILES: [Nb]123456(N(CCC[NH2]1)[Si]([c]13[cH]4[cH]5[cH]6[cH]21)(C)C)(Cl)(Cl)Cl
• Title of publication: Cyclopentadienyl-Silyl-Amido Niobium Complexes Prepared by a Transmetalation Reaction Using Ti{η5-C5H4SiMe2-η-N(CH2)2NRR‘}Cl2†
• Authors of publication: Maestre, M. Carmen; Tabernero, Vanessa; Mosquera, Marta E. G.; Jiménez, Gerardo; Cuenca, Tomás
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 24
• Pages of publication: 5853
• a: 14.3848 ± 0.0015 Å
• b: 7.5381 ± 0.0007 Å
• c: 15.2675 ± 0.0013 Å
• α: 90°
• β: 110.582 ± 0.01°
• γ: 90°
• Cell volume: 1549.8 ± 0.3 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0568
• Residual factor for significantly intense reflections: 0.0326
• Weighted residual factors for significantly intense reflections: 0.0633
• Weighted residual factors for all reflections included in the refinement: 0.0687
• Goodness-of-fit parameter for all reflections included in the refinement: 1.006
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No