Information card for entry 4076144

Structure parameters

• Formula: C88 H88 B2 Cl4 F8 O4 P4 Rh2 Zr2
• Calculated formula: C88 H84 B2 Cl4 F8 O4 P4 Rh2 Zr2
• Title of publication: Flexible Building Blocks for Transition Metal Early−Late Chemistry. Synthesis of Heterobimetallic Tetranuclear Metallomacrocycles
• Authors of publication: Álvarez-Vergara, M. Carmen; Casado, Miguel A.; Martín, M. Luisa; Lahoz, Fernando J.; Oro, Luis A.; Pérez-Torrente, Jesús J.
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 24
• Pages of publication: 5929
• a: 19.703 ± 0.002 Å
• b: 17.9741 ± 0.0018 Å
• c: 25.627 ± 0.003 Å
• α: 90°
• β: 110.236 ± 0.002°
• γ: 90°
• Cell volume: 8515.5 ± 1.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.143
• Residual factor for significantly intense reflections: 0.0963
• Weighted residual factors for significantly intense reflections: 0.2038
• Weighted residual factors for all reflections included in the refinement: 0.222
• Goodness-of-fit parameter for all reflections included in the refinement: 1.147
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No