Information card for entry 4076167

Structure parameters

• Formula: C73 H108 Al2 N18 Si2
• Calculated formula: C73 H108 Al2 N18 Si2
• SMILES: [Si]1(N([Al]2([N](=C(C)C=C(N2c2c(cccc2C(C)C)C(C)C)C)c2c(cccc2C(C)C)C(C)C)N=N#N)[Si](N1[Al]1([N](=C(C)C=C(N1c1c(cccc1C(C)C)C(C)C)C)c1c(cccc1C(C)C)C(C)C)N=N#N)(N=N#N)C(C)(C)C)(N=N#N)C(C)(C)C.c1(ccccc1)C
• Title of publication: Syntheses and Structural Characterization of a LAl(N3)N[μ-Si(N3)(tBu)]2NAl(N3)L and a Monomeric Aluminum Hydride Amide LAlH(NHAr) (L = HC[(CMe)(NAr)]2, Ar = 2,6-iPr2C6H3)
• Authors of publication: Zhu, Hongping; Yang, Zhi; Magull, Jörg; Roesky, Herbert W.; Schmidt, Hans-Georg; Noltemeyer, Mathias
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 26
• Pages of publication: 6420
• a: 12.9225 ± 0.0006 Å
• b: 16.5684 ± 0.0008 Å
• c: 19.7508 ± 0.0009 Å
• α: 102.657 ± 0.004°
• β: 99.836 ± 0.004°
• γ: 99.243 ± 0.004°
• Cell volume: 3978.1 ± 0.3 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0837
• Residual factor for significantly intense reflections: 0.0629
• Weighted residual factors for significantly intense reflections: 0.177
• Weighted residual factors for all reflections included in the refinement: 0.1925
• Goodness-of-fit parameter for all reflections included in the refinement: 1.082
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No