Information card for entry 4076255

Structure parameters

• Formula: C80 H172 O8 P4 Sn4
• Calculated formula: C80 H172 O8 P4 Sn4
• Title of publication: Reactions ofn-Bu2SnO and (n-Bu3Sn)2O with 1,1,2,3,3-Pentamethyltrimethylene Phosphinic Acid: Synthesis and X-ray Crystal Structures of a Novel Spirocyclic Coordination Polymer and a 16-Membered Inorganic Macrocycle
• Authors of publication: Chandrasekhar, Vadapalli; Baskar, Viswanathan; Steiner, Alexander; Zacchini, Stefano
• Journal of publication: Organometallics
• Year of publication: 2004
• Journal volume: 23
• Journal issue: 6
• Pages of publication: 1390
• a: 19.2108 ± 0.0008 Å
• b: 19.2108 ± 0.0008 Å
• c: 13.0532 ± 0.0007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4817.3 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 86
• Hermann-Mauguin space group symbol: P 42/n :2
• Hall space group symbol: -P 4bc
• Residual factor for all reflections: 0.0627
• Residual factor for significantly intense reflections: 0.0449
• Weighted residual factors for significantly intense reflections: 0.1133
• Weighted residual factors for all reflections included in the refinement: 0.1296
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No