Information card for entry 4076301

Structure parameters

• Formula: C106.5 H38.75 Cl2.25 Co F6 P3 Pd
• Calculated formula: C106.5 H38.75 Cl2.25 Co F6 P3 Pd
• Title of publication: Synthetic and Structural Studies on the Transition-Metal Fullerene Complexes (η2-C60)M[(η5-Ph2PC5H4)2Ru] and (η2-C60)M[(η5-Ph2PC5H4)2Co]+(PF6)-(M = Pd, Pt) and the Related Compound {[η5-Ph2P(O)C5H4]2Co}+(PF6)-
• Authors of publication: Song, Li-Cheng; Yu, Guang-Ao; Su, Fu-Hai; Hu, Qing-Mei
• Journal of publication: Organometallics
• Year of publication: 2004
• Journal volume: 23
• Journal issue: 18
• Pages of publication: 4192
• a: 14.747 ± 0.004 Å
• b: 24.155 ± 0.009 Å
• c: 19.768 ± 0.006 Å
• α: 90°
• β: 90.541 ± 0.01°
• γ: 90°
• Cell volume: 7041 ± 4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1412
• Residual factor for significantly intense reflections: 0.0642
• Weighted residual factors for significantly intense reflections: 0.1225
• Weighted residual factors for all reflections included in the refinement: 0.1563
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No