Information card for entry 4076491

Structure parameters

• Common name: L'(NEt2)Al(NEt2)Li(THF)
• Formula: C34 H60 Al Li N4 O
• Calculated formula: C34 H60 Al Li N4 O
• SMILES: [Al]12([N]3([Li]([N]2(CC)CC)([N](C3c2n1c(cc2)C(C)(C)C)(CC)CC)[O]1CCCC1)c1c(cccc1C(C)C)C(C)C)C
• Title of publication: Syntheses and Reactions of Derivatives of (Pyrrolylaldiminato)germanium(II) and -Aluminum(III)
• Authors of publication: Yang, Ying; Zhao, Na; Zhu, Hongping; Roesky, Herbert W.
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 5
• Pages of publication: 1958
• a: 14.935 ± 0.003 Å
• b: 13.868 ± 0.003 Å
• c: 17.071 ± 0.003 Å
• α: 90°
• β: 91.06 ± 0.03°
• γ: 90°
• Cell volume: 3535.1 ± 1.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0776
• Residual factor for significantly intense reflections: 0.0682
• Weighted residual factors for significantly intense reflections: 0.2031
• Weighted residual factors for all reflections included in the refinement: 0.213
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No