Information card for entry 4076643

Structure parameters

• Formula: C65.5 H94 Cl4 N4 O Yb2
• Calculated formula: C65.5 H93.5 Cl4 N4 O Yb2
• Title of publication: Synthesis, Reactivity, and Structure of Mixed-Ligand Ytterbium Complexes Supported by β-Diketiminate
• Authors of publication: Yao, Yingming; Zhang, Yong; Shen, Qi; Yu, Kaibei
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 5
• Pages of publication: 819
• a: 19.951 ± 0.004 Å
• b: 13.918 ± 0.002 Å
• c: 24.257 ± 0.005 Å
• α: 90°
• β: 98.71 ± 0.01°
• γ: 90°
• Cell volume: 6658 ± 2 ų
• Cell temperature: 299 ± 2 K
• Ambient diffraction temperature: 299 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0915
• Residual factor for significantly intense reflections: 0.0405
• Weighted residual factors for significantly intense reflections: 0.0561
• Weighted residual factors for all reflections included in the refinement: 0.0639
• Goodness-of-fit parameter for all reflections included in the refinement: 0.79
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No