Information card for entry 4076746

Structure parameters

• Formula: C47 H44 B Cl N2 O2.5 Os P2
• Calculated formula: C47.5 H44 B Cl N2 O2.5 Os P2
• Title of publication: Tethered Osmium Boryl Complexes from the Reaction of Os(BCl2)Cl(CO)(PPh3)2with 2-Hydroxypyridine
• Authors of publication: Rickard, Clifton E. F.; Roper, Warren R.; Williamson, Alex; Wright, L. James
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 8
• Pages of publication: 1714
• a: 9.4822 ± 0.0001 Å
• b: 11.5729 ± 0.0001 Å
• c: 21.3401 ± 0.0001 Å
• α: 82.024 ± 0.001°
• β: 81.023 ± 0.001°
• γ: 67.463 ± 0.0001°
• Cell volume: 2128.44 ± 0.03 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0249
• Residual factor for significantly intense reflections: 0.0216
• Weighted residual factors for significantly intense reflections: 0.0508
• Weighted residual factors for all reflections included in the refinement: 0.0524
• Goodness-of-fit parameter for all reflections included in the refinement: 1.087
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No