Information card for entry 4076794

Structure parameters

• Formula: C74 H54 Ag Cl5 F10 O4 P4 Pt3
• Calculated formula: C74 H54 Ag Cl5 F10 O4 P4 Pt3
• Title of publication: Synthesis of Mixed-Valence Platinum Triangulo Clusters [Pt3(μ-PPh2)2(μ-C6F5)(C6F5)(PPh2R)2] (R = Ph, Me, Et). Crystal Structures of [Pt3(μ-PPh2)2(μ-C6F5)(C6F5)(PPh3)2] and [Pt3(μ-AgOClO3)(μ-PPh2)2(μ-C6F5)(C6F5)(PPh3)2]†
• Authors of publication: Falvello, Larry R.; Forniés, Juan; Fortuño, Consuelo; Durán, Fernando; Martín, Antonio
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 11
• Pages of publication: 2226
• a: 11.4288 ± 0.0007 Å
• b: 14.1307 ± 0.0006 Å
• c: 22.4596 ± 0.0012 Å
• α: 93.525 ± 0.007°
• β: 90.552 ± 0.016°
• γ: 94.159 ± 0.01°
• Cell volume: 3610.4 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0485
• Residual factor for significantly intense reflections: 0.034
• Weighted residual factors for significantly intense reflections: 0.0898
• Weighted residual factors for all reflections included in the refinement: 0.0964
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No