Information card for entry 4076820

Structure parameters

• Formula: C74 H77 B11 Cl4 P4 Rh2
• Calculated formula: C74 H77 B11 Cl4 P4 Rh2
• Title of publication: Rhodium Phosphines Partnered with the Carborane Monoanions [CB11H6Y6]-(Y = H, Br). Synthesis and Evaluation as Alkene Hydrogenation Catalysts
• Authors of publication: Rifat, Adem; Patmore, Nathan J.; Mahon, Mary F.; Weller, Andrew S.
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 14
• Pages of publication: 2856
• a: 20.572 ± 0.0007 Å
• b: 16.362 ± 0.0005 Å
• c: 21.557 ± 0.0008 Å
• α: 90°
• β: 90.699 ± 0.002°
• γ: 90°
• Cell volume: 7255.5 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1886
• Residual factor for significantly intense reflections: 0.0827
• Weighted residual factors for significantly intense reflections: 0.1358
• Weighted residual factors for all reflections included in the refinement: 0.1742
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No