Information card for entry 4076892

Structure parameters

• Formula: C46.5 H49 P3 Pd
• Calculated formula: C46.5 H43 P3 Pd
• Title of publication: Palladium(II) Terminal Phosphido Complexes Derived from Cyclometalated Dimesitylphosphine: Synthesis, Structure, and Low-Barrier Phosphorus Inversion
• Authors of publication: Zhuravel, Michael A.; Glueck, David S.; Zakharov, Lev N.; Rheingold, Arnold L.
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 15
• Pages of publication: 3208
• a: 9.4352 ± 0.0017 Å
• b: 23.389 ± 0.004 Å
• c: 18.249 ± 0.003 Å
• α: 90°
• β: 90.213 ± 0.004°
• γ: 90°
• Cell volume: 4027.2 ± 1.2 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0611
• Residual factor for significantly intense reflections: 0.0402
• Weighted residual factors for significantly intense reflections: 0.0987
• Weighted residual factors for all reflections included in the refinement: 0.1131
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No