Information card for entry 4076934

Structure parameters

• Common name: compound 3c * 0.5CH2Cl2
• Formula: C34.5 H33 Cl Fe O4 Os
• Calculated formula: C34.5 H33 Cl Fe O4 Os
• Title of publication: Macrocyclic Di- and Tetranuclear Osmacycloferrocenophanes†,1
• Authors of publication: Lindner, Ekkehard; Ayasse, Christoph S.; Eichele, Klaus; Steimann, Manfred
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 20
• Pages of publication: 4217
• a: 6.2833 ± 0.0017 Å
• b: 16.437 ± 0.003 Å
• c: 29.161 ± 0.004 Å
• α: 90°
• β: 92.244 ± 0.017°
• γ: 90°
• Cell volume: 3009.4 ± 1.1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0758
• Residual factor for significantly intense reflections: 0.0463
• Weighted residual factors for significantly intense reflections: 0.0974
• Weighted residual factors for all reflections included in the refinement: 0.1091
• Goodness-of-fit parameter for all reflections included in the refinement: 1.007
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No