Information card for entry 4077047

Structure parameters

• Formula: C62 H70 B9 Cl4 P4 Rh Ru S
• Calculated formula: C62 H70 B9 Cl4 P4 Rh Ru S
• Title of publication: Chemistry of a Metallathiaborane Cluster. 5.†Reaction of [8,8-(η2-dppm)-8-(η1-dppm)-nido-8,7-RhSB9H10] and Its Derivatives with Organotransition-Metal Reagents
• Authors of publication: Volkov, Oleg; Rath, Nigam P.; Barton, Lawrence
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 25
• Pages of publication: 5505
• a: 14.7117 ± 0.0007 Å
• b: 20.0133 ± 0.001 Å
• c: 22.9074 ± 0.0012 Å
• α: 90°
• β: 107.165 ± 0.003°
• γ: 90°
• Cell volume: 6444.2 ± 0.6 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1296
• Residual factor for significantly intense reflections: 0.0612
• Weighted residual factors for significantly intense reflections: 0.0885
• Weighted residual factors for all reflections included in the refinement: 0.1044
• Goodness-of-fit parameter for all reflections included in the refinement: 1.012
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No