Information card for entry 4077049

Structure parameters

• Formula: C50 H41 B F4 P2 Ru
• Calculated formula: C50 H41 B F4 P2 Ru
• Title of publication: Synthesis and Properties of the Indenyl Ruthenium(II) Complex [Ru{(E)-η1-C(C⋮CPh)CHPh}(η5-C9H7)(κ2-P-dppm)] (dppm = bis(diphenylphosphino)methane). An Organometallic Intermediate in the Catalytic Dimerization of Phenylacetylene
• Authors of publication: Bassetti, Mauro; Marini, Silvia; Díaz, Josefina; Gamasa, M. Pilar; Gimeno, José; Rodríguez-Álvarez, Yolanda; García-Granda, Santiago
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 22
• Pages of publication: 4815
• a: 20.638 ± 0.004 Å
• b: 11.067 ± 0.005 Å
• c: 18.819 ± 0.005 Å
• α: 90°
• β: 95.32 ± 0.01°
• γ: 90°
• Cell volume: 4280 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1531
• Residual factor for significantly intense reflections: 0.0554
• Weighted residual factors for significantly intense reflections: 0.139
• Weighted residual factors for all reflections included in the refinement: 0.1741
• Goodness-of-fit parameter for all reflections included in the refinement: 1.003
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No