Information card for entry 4077053

Structure parameters

• Formula: C60.5 H79 N2 Ta
• Calculated formula: C60.5 H79 N2 Ta
• Title of publication: Tantalum Alkyl and Silyl Complexes of the Bulky (Terphenyl)imido Ligand [2,6-(2,4,6-Me3C6H2)2C6H3N]2-([Ar*N]2-). Generation and Reactivity of [(Ar*N)(Ar*NH)Ta(H)(OSO2CF3)], Which Reversibly Transfers Hydride to an Aromatic Ring of the Arylamide Ligand
• Authors of publication: Gavenonis, John; Tilley, T. Don
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 25
• Pages of publication: 5549
• a: 10.9435 ± 0.0009 Å
• b: 43.319 ± 0.004 Å
• c: 12.4363 ± 0.001 Å
• α: 90°
• β: 115.977 ± 0.002°
• γ: 90°
• Cell volume: 5299.9 ± 0.8 ų
• Cell temperature: 159 ± 2 K
• Ambient diffraction temperature: 159 ± 2 K
• Number of distinct elements: 4
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0793
• Residual factor for significantly intense reflections: 0.0506
• Weighted residual factors for all reflections: 0.0895
• Weighted residual factors for significantly intense reflections: 0.0791
• Goodness-of-fit parameter for all reflections: 0.942
• Goodness-of-fit parameter for significantly intense reflections: 0.94
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No