Information card for entry 4077064

Structure parameters

• Formula: C51 H113 Cl2 O4 P4 Ru4 Si2
• Calculated formula: C51 H106 Cl2 O4 P4 Ru4 Si2
• Title of publication: Trans Additions of Silanes to 1-Alkynes Catalyzed by Ruthenium Complexes: Role of in Situ Formed Polynuclear Aggregates
• Authors of publication: Martín, Marta; Sola, Eduardo; Lahoz, Fernando J.; Oro, Luis A.
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 20
• Pages of publication: 4027
• a: 22.567 ± 0.0018 Å
• b: 12.8393 ± 0.001 Å
• c: 26.88 ± 0.002 Å
• α: 90°
• β: 111.602 ± 0.002°
• γ: 90°
• Cell volume: 7241.3 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1126
• Residual factor for significantly intense reflections: 0.0572
• Weighted residual factors for significantly intense reflections: 0.1191
• Weighted residual factors for all reflections included in the refinement: 0.1325
• Goodness-of-fit parameter for all reflections included in the refinement: 0.867
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No