Information card for entry 4077066

Structure parameters

• Formula: C44.67 H72 O17.33 P5.33 Sn2.67
• Calculated formula: C44.6667 H72 O17.3333 P5.33333 Sn2.66667
• Title of publication: Synthesis of a Tetranuclear Organooxotin Cage by Debenzylation Reactions: X-ray Crystal Structure of [(PhCH2)2Sn2O(O2P(OH)-t-Bu)4]2
• Authors of publication: Chandrasekhar, Vadapalli; Baskar, Viswanathan; Steiner, Alexander; Zacchini, Stefano
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 21
• Pages of publication: 4528
• a: 21.774 ± 0.004 Å
• b: 24.507 ± 0.005 Å
• c: 16.699 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8911 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 52
• Hermann-Mauguin space group symbol: P n n a
• Hall space group symbol: -P 2a 2bc
• Residual factor for all reflections: 0.041
• Residual factor for significantly intense reflections: 0.0233
• Weighted residual factors for significantly intense reflections: 0.0649
• Weighted residual factors for all reflections included in the refinement: 0.072
• Goodness-of-fit parameter for all reflections included in the refinement: 1.082
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No