Information card for entry 4077226

Structure parameters

• Formula: C22 H31 B10 Cl P2 Pd Sn
• Calculated formula: C22 H31 B10 Cl P2 Pd Sn
• Title of publication: Synthesis and Reactivity of Organotin Compounds Containing the C,P-Chelatingo-Carboranylphosphino Ligand [o-C2B10H10PPh2-C,P](CabC,P). X-ray Structures of (CabC,CH2P)SnMe2Br, [(CabC,P)SnMe2]2Pd, and [(CabC,P)SnMe2]Pd(PEt3)Cl
• Authors of publication: Lee, Taegweon; Lee, Soon W.; Jang, Ho G.; Kang, Sang Ook; Ko, Jaejung
• Journal of publication: Organometallics
• Year of publication: 2001
• Journal volume: 20
• Journal issue: 4
• Pages of publication: 741
• a: 12.8395 ± 0.001 Å
• b: 15.0348 ± 0.0015 Å
• c: 17.2473 ± 0.0013 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3329.4 ± 0.5 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 7
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0613
• Residual factor for significantly intense reflections: 0.0462
• Weighted residual factors for significantly intense reflections: 0.1167
• Weighted residual factors for all reflections included in the refinement: 0.1264
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No