Information card for entry 4077276

Structure parameters

• Formula: C26 H56 Cl Ir Sb2
• Calculated formula: C26 H56 Cl Ir Sb2
• Title of publication: Square-Planar Bis(triisopropylstibine)(olefin)iridium(I) Complexes and Their Rearrangement to (η3-Allyl)hydridoiridium(III) Isomers
• Authors of publication: Ortmann, Dagmara A.; Gevert, Olaf; Laubender, Matthias; Werner, Helmut
• Journal of publication: Organometallics
• Year of publication: 2001
• Journal volume: 20
• Journal issue: 9
• Pages of publication: 1776
• a: 16.985 ± 0.009 Å
• b: 20.15 ± 0.009 Å
• c: 9.374 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3208 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.082
• Residual factor for significantly intense reflections: 0.0407
• Weighted residual factors for all reflections: 0.1136
• Weighted residual factors for significantly intense reflections: 0.0864
• Goodness-of-fit parameter for all reflections: 1.051
• Goodness-of-fit parameter for significantly intense reflections: 1.003
• Diffraction radiation wavelength: 0.7093 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No