Information card for entry 4077336

Structure parameters

• Formula: C148 H264 B40 Na8 O20 Si4 Yb3
• Calculated formula: C74 H122 B20 Na4 O10 Si2 Yb1.5
• Title of publication: A Novel Full-Sandwich Lanthanacarborane Complex Bearing anη7-Carboranyl Ligand, {{[η7-Me2Si(C13H9)(C2B10H11)]2YbIII}2YbII}{Na8(THF)20}
• Authors of publication: Wang, Shaowu; Li, Hung-Wing; Xie, Zuowei
• Journal of publication: Organometallics
• Year of publication: 2001
• Journal volume: 20
• Journal issue: 18
• Pages of publication: 3842
• a: 14.3481 ± 0.0016 Å
• b: 16.0906 ± 0.0018 Å
• c: 21.811 ± 0.002 Å
• α: 106.145 ± 0.002°
• β: 105.365 ± 0.002°
• γ: 98.694 ± 0.002°
• Cell volume: 4524.5 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1799
• Residual factor for significantly intense reflections: 0.074
• Weighted residual factors for significantly intense reflections: 0.1799
• Weighted residual factors for all reflections included in the refinement: 0.2292
• Goodness-of-fit parameter for all reflections included in the refinement: 0.88
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No